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  • 1.
    Khaji, Zahra
    et al.
    Uppsala University.
    Sturesson, Peter
    Swedish Defence University, Department of Military Studies, Military-Technology Division. Uppsala University.
    Hjort, Klas
    Uppsala University.
    Klintberg, Lena
    Uppsala University.
    Thornell, Greger
    Uppsala University.
    Investigation of the storage and release of oxygen in a Cu-Pt element of a high-temperature microcombustor2014In: Journal of Physics Conference Series, Institute of Physics Publishing (IOPP), 2014Conference paper (Refereed)
    Abstract [en]

    A miniature combustor for converting organic samples into CO2 with application in carbon isotopic measurements has been manufactured and evaluated. The combustor was made of High-Temperature Co-fired Ceramic (HTCC) alumina green tapes. The device has a built-in screen printed heater and a temperature sensor made of platinum, co-sintered with the ceramic. A copper oxide oxygen supply was added to the combustor after sintering by in-situ electroplating of copper on the heater pattern followed by thermal oxidation. Scanning Electron Microscopy (SEM), Energy Dispersive Spectroscopy (EDS) and Thermal Gravimetric Analysis (TGA) were used to study electroplating, oxidation and the oxide reduction processes. The temperature sensor was calibrated by use of a thermocouple. It demonstrates a temperature coefficient resistance of 4.66×10−3/°C between 32 and 660 °C. The heat characterization was done up to 1000 °C by using IR thermography, and the results were compared with the data from the temperature sensor. Combustion of starch confirmed the feasibility of using copper oxide as the source of oxygen of combustion.

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